Determination of primary aromatic amines with MS detection
Article number: VEV0043J
Details
| Method | UHPLC |
|---|---|
| Eluent | A: H2O + 0.1 % FA (formic acid) B: Methanol + 0,1 % FA |
| Gradient | 0.0 – 3.0 min 20 - 40 % B 3.0 – 3.1 min 40 - 100 % B 3.1 – 5.0 min 100 % B |
| Flow rate | 0.2 ml/min |
| Injection volume | 10 µl |
| Temperature | 40 °C |
| Detection | MSQ Plus, ESI pos. mode, Needle 1 kV, coneV 20 V, Probe temperature 200 °C full scan m/z = 80 – 170 |
| Substances | Aniline, 2-Anisidine, o-Toluidine, 3-Chloro-4-methoxyaniline, 2,4-Dimethylaniline |
| Chromatogram | 1. Aniline, 2. 2-Anisidine, 3. o-Toluidine, 4. 3-Chloro-4-methoxyaniline, 5. 2,4-Dimethylaniline |
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Vertex Plus Column 100 x 2 mm BlueOrchid 175-1.8 C18 | 10BI181BOE | Vertex Plus Column 100 x 2 mm BlueOrchid 175-1.8 C18 |
Technical data are subject to change without notice.
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