1. Aldicarb sulphoxide; 2. Aldicarb sulphone; 3. Oxamyl; 4. Methomyl; 5. 3-Hydroxycarbofuran; 6. Aldicarb; 7. Propoxur; 8. Carbofuran; 9. Carbaryl; 10. 1- Naphtol; 11. Methiocarb; 12. BDMC
Determination of Carbamate Insecticides by HPLC with post-column derivatization
Article number: VEV0012J
| Method | HPLC |
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| Eluent | A: Water B: Methanol
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| Gradient | 0 – 0.5 min 82% A 0.5 – 29 min 82% – 30% A 29 – 31 min 100% B, column rinsing 31 – 36 min 82% A, re-equalibration
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| Flow rate | 1.0 ml/min |
| Mode | RP Mode |
| Injection volume | 10 µl |
| Temperature | 42 °C |
| Additional procedure | Post-column derivatization, two step reaction 1st Reactor (500 µl): 100 °C for first derivatization step with NaOH 2nd Reactor (150 µl): ambient with OPA and 2-mercaptoethanol derivative
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| Detection | Fluorescence: excitation 330 nm, emission 465 nm |
| Substances | Aldicarb, Aldicarb sulphoxide, Aldicarb sulphone, BDMC, Carbaryl, Carbofuran, 3-Hydroxycarbofuran, Methiocarb, Methomyl, 1-Naphtol, Oxamyl, Propoxur |
| Key words | Carbamates, Insecticides |
| Chromatogram | 1. Aldicarb sulphoxide 2. Aldicarb sulphone 3. Oxamyl 4. Methomyl 5. 3-Hydroxycarbofuran 6. Aldicarb 7. Propoxur 8. Carbofuran 9. Carbaryl 10. 1- Naphtol 11. Methiocarb 12. BDMC
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Chromatogram VEV0012J | 1. Aldicarb sulphoxide; 2. Aldicarb sulphone; 3. Oxamyl; 4. Methomyl; 5. 3-Hydroxycarbofuran; 6. Aldicarb; 7. Propoxur; 8. Carbofuran; 9. Carbaryl; 10. 1- Naphtol; 11. Methiocarb; 12. BDMC |
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VertexPlus Column 250 x 4.6 mm Eurospher 100-5 C18 | 25EE181ESJ | VertexPlus Column 250 x 4.6 mm Eurospher 100-5 C18 |
Technical data are subject to change without notice.